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WEB Ti3SiC2- and Ti3AlC2-based ceramics synthesis by spark plasma sintering of preceramic paper

Monday (02.03.2020)
07:41 - 07:41 Poster Room
Part of:
- Poster *web*Smoothing of additive manufactured parts using ns-pulsed laser source 1 Dipl.-Ing. Florian Kuisat
- Poster TBA -
- Poster *web*Combustion Synthesis of High Entropy Alloys thin films 1 Dr. Anni Wang
- Poster *web*Surface macro-smoothing and micro-structuring of additive manufactured components by using DLIP technique for controlling wetting characteristics 1 Dipl.-Ing. Florian Kuisat
- Poster *web*Influence of embedding materials on heat transfer and ignition transfer time in heterogeneous reactive material system 1 Mostafa Baloochi
- Poster TBA -
- Poster *web*Self reactive joining process with multilayer foils in lap joint configuration 1 Marcus Glaser
- Poster *web*Thermodynamics and kinetics of phase formation in magnetron-sputtered Ni/Al multilayer thin films with nanoscale morphology 1 Sascha Sebastian Riegler
- Poster *web*Femtosecond laser approach to cut Ni/Al reactive foils without ignition of a self-propagation reaction 1 Maria Amelia Martins
- Poster *web*Effect of preparation angle on atom probe tomography of reactive multilayers 1 Christian Schäfer
- Poster *web*Reactive Ni/Al multilayers with 3D Morphologies 1 Konrad Jaekel
- Poster *web*Synchrotron radiation X-ray powder diffraction and magnetometric study of natural and synthetic terms of the stannite-kesterite pseudobinary system in the low temperature regime (5-275 K) 1 Dr. Francesco Di Benedetto
- Poster *web*Coating and Drying of Sodium-Ion-Battery Electrodes 1 Julian Klemens
- Poster *web*Analytical prediction model for Direct Laser Interference Patterning 1 Dr. Bogdan Voisiat
- Poster *web*CFD Analysis of joining processes using reactive multilayers on native surface morphologies of microelectronic substrates 1 Erik Wiss
- Poster *web*Top-Hat profile in Direct Laser Interference Patterning: Is it worth it? 1 Mikhael El-Khoury
- Poster *web*Laser-based (“2D”) surface treatment of lithium-ion battery electrodes to improve the rate capability 1 Jens Sandherr
- Poster *web*Microstructure investigation of superconducting NbN thin films on copper 1 Dipl.-Ing. Ying Li
- Poster TBA -
- Poster *web*Laser functionalized PEEK-based coating systems to minimize friction and wear 1 Dr. Tim Kunze
- Poster *web*Structure and Dynamics in a Layered Na-ion Battery Cathode 1 Euan Bassey
- Poster *web*Electrode-Processing using porous nano-structured Na3V2(PO4)3 (NVP) for Sodium-Ion Batteries 1 Luca Schneider
- Poster TBA -
- Poster *web*Experimental Approach for Phase Diagram determination of Li alloys 1 Joel Fels
- Poster *web*Process Integration of Few-Layer MoS2 into a-Si:H Heterojunction pin-Photodiodes for extended Infrared Detection 1 Charles Otieno Ogolla
- Poster *web*Ti3SiC2- and Ti3AlC2-based ceramics synthesis by spark plasma sintering of preceramic paper 1 Elizaveta Sedanova
- Poster *web*Overheating microstructural study of nickel-based superalloys from turbine blades of aircraft engines 1 Dr. Ana Pastor
- Poster *web*Electrochemical thermodynamics of Lithium Batteries and their materials 1 Prof. Dr. Hans Jürgen Seifert
- Poster *web*Corrosion Analysis of a 316L Stainless Steel Gas Outlet Sealed with a Copper Ring Used in the CO2 Methanation Process 1 Ananya Prechavut
- Poster *web*Self-propagating reaction of structured reactive Al/Ni multilayers 1 Yesenia Sauni
- Poster *web*3D structured electrodes for Li-ion batteries using open porous metal foams as current collector for high energy application 1 Jonas Oehm
- Poster *web*Novel air stable single source precursor for homogeneous crystalline TiS2 thin films 1 Anja Sutorius
- Poster *web*Synthesis of nickel-copper composite with controllable nanostructure through facile solvent control as positive electrode for high-performance supercapacitors 1 Dr. Damin Lee
- Poster *web*Towards understanding response generation in conductometric gas sensors 1 Stefan Kucharski
- Poster Effects of 3D electrode design on high-energy silicon-graphite anode materials 1 Yijing Zheng

Session -F: Functional Materials, Surfaces, and Devices
Belongs to:
Topic X: Poster Session

Titanium silicon carbide (Ti3SiC2) and titanium aluminum carbide (Ti3AlC2) are well-studied compounds among the nano-laminated Mn+1AX n ternary compounds, where М – transition metal, А – IIIA-IVA element of the periodic table, Х – carbon or nitrogen. These compounds usually exhibit a unique combination of both ceramic and metallic properties. A large number of MAX phases have been synthesized and the potential for their application has been demonstrated for different industries, in particular, they are promising materials for aerospace and transport applications. Porous MAX phase including paper-derived ceramics can be used for high-temperature filtering systems, energy-saving components, electrodes or sensor ceramics.

Spark plasma sintering (SPS) can be used for the synthesis of the MAX phase –based materials due to its potential for manufacturing dense materials at considerably low temperature in a relatively short time. In the present work, we suggested a novel technique to fabricate MAX-phase based materials by application of preceramic papers as preforms for SPS. The manufacturing of preceramic paper is one of the important technological approaches for shaping materials. The preforms can be shaped into multilayer laminates or more complex shapes. Additionally, the porosity of the composites can be controlled by the preceramic paper composition and sintering parameters.

The current work presents the results on the sintering of paper-derived Ti3SiC2– and Ti3AlC2–based composites. The influence of spark plasma sintering parameters on phase composition and microstructure was analyzed by X-ray diffraction (XRD) and scanning electron microscopy, respectively. In addition, energy-dispersive X-ray spectroscopy was carried out to analyze the distribution of elements and the phase arrangement depending on the sintering temperature. The influence of SPS parameters on the formation of phase composition, microstructure and mechanical properties of the sintered composites was discussed.

Elizaveta Sedanova
National Research Tomsk Polytechnic University
Additional Authors:
  • Egor Kashkarov
    National Research Tomsk Polytechnic University
  • Maxim Syrtanov
    National Research Tomsk Polytechnic University
  • Prof. Andrey Lider
    National Research Tomsk Polytechnic University
  • Prof. Nahum Travitzky
    Friedrich-Alexander-Universität Erlangen-Nürnberg


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